Determined syn8/31/2023 Those three reactions we’ll look at today are addition of HBr, bromination with Br 2, and hydrogenation with Pd-C and H 2. We’re going to look at three key reactions of alkenes and see how they each demonstrate a different pattern of stereochemistry in addition reactions. This post is about the second key theme in addition reactions of alkenes: stereochemistry. In the last post on alkene addition reactions, we discussed one of the two key themes to look for in addition reactions: regiochemistry (in other words – what is the favored direction in which the pi-bond breaks). A Collection Of Observations That Nobody Predicted Ahead Of Time Until They Did The Experiment Summary: Stereoselectivity In Alkene Addition Reactionsġ.Hydrogenation Of Alkenes With Pd-C And H 2 Is Selective For Addition Stereochemistry.Addition Of Bromine To Alkenes Is Stereoseletvie, Giving “Anti” Addition Stereochemistry.Addition Of H-Br To Alkenes Is Not Stereoselective, And Gives A Roughly Equal Mixture Of “Syn” And “Anti” Products.A Collection of Observations On Reaction Alkene Addition Stereochemistry That Nobody Predicted Ahead Of Time.An example of this is bromination with Br2 or chlorination with Cl2 In a second pattern, the addition reaction gives anti products. ![]() An example is the addition of H-Br to alkenes ![]() In one pattern, the addition reaction gives a mixture of syn and anti products.In addition to the regioselectivity of an addition reaction (often summarized by Markovnikov’s Rule) there are three important patterns for the stereoselectivity of reactions.To keep them all straight, it is helpful to divide them into families depending on the pattern of bonds that form and break. There are a large number of alkene addition reactions.Stereoselectivity In Alkene Addition Reactions: “Syn” vs “Anti”
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The problem with these bones is that bones of dead animals and Haram animals or even humans get entry into these bones. They become naturally degreased and dry in the fields and many Kosher groups prefer these over slaughter house bones. Field bones are picked up by scavengers from the fields or garbage and sold to junk dealers in South Asia. It is Halal by its nature but is very expensive. Fish gelatin is available in small quantities. Moreover a very small amount of calf and beef gelatin comes from animals slaughtered by Muslims. Calf skin and beef bone gelatin are readily available but cost more than the pork gelatin for an equivalent gel grade. Most common type of gelatin used by the food industry is pork gelatin, due to its price advantage. This soupy solution is then dried into sheets or noodles and crushed into small pieces that look like sugar. Gelatin is made by simmering the pieces of skins or bones in hot water to a solution that looks like chicken soup. Commercially, common sources of gelatin are Pork skins, Calf skins, Beef bones, Fish skins, and Field bones. Gelatin is a product of animal origin only, extracted from bones and skins of many animals or fish. In Jell-O dessert, gelatin is not listed as Kosher gelatin but the package (Jell-O) is labeled as Kosher, designated with letter “K.” Still in other products that are labeled as Kosher, gelatin may be present but not listed on the label. ![]() In yogurt, it is listed as Kosher gelatin in the ingredients on the label. IFANCA frequently receives inquiries about gelatin, especially Kosher gelatin. Cobalt 60 information8/31/2023 Of these, 31 patients were treated with a dose of 2000 r (estimated tumor dose) in about 21/2% to 3 weeks. All patients were treated by a single course of consecutive daily sessions, the majority with x rays (200 to 250 kv range). In 99 patients the diagnosis was chromophobe adenoma and in 31 eosinophilic adenoma. (BBB) « lessįrom 1940 to 1959, 130 patients with pituitery adenomas were treated with external radiation. In the 110 cases local tumor disappearance was noted in 60% to 80%, depending on whether an optimistic or pessimistic view was taken of those cases with still uncertain status. It is concluded that the pressure vessel allows treatment of advanced tumors in practically all sites without seriously limiting the application of x-ray fields which would be normally chosen with conventional megavoltage therapy. Bilateral myringotomy produced temporary deafness, usually unilaterai, in approximately 20% of the cases, and oniy four patients have any residual deafness. ![]() The resolution was far superior with barotherapy. In three patients, comparison was possible of the tumor resolution produced by the barotherapy technique with the resolution produced when similar dosage was given in air to a regional metastasis later appearing. Definite local recurrence of tumor within the treated volume was confirmed in only a few cases. The use of antibiotics, conticosteroids, and triiodothyronine did not infiuence progression. Delayed necroses appeared commonly five months after completing treatment in those cases treated with high doses who developed the most intense mucous membrane reactions even though healing was almost complete 2 to 3 months after treatment. ![]() Tumor resolution with the various dosage schemes employed was very satisfactory and often dramatic. Skin reactions, on the other hand, seemed to parallel the dosage received on the skin and not to be aggravated by oxygenation effects. Animal lab studies lended suppont to this conclusion. Experience with similar large doses delivered in air, compared with those used with barotherapy, suggests that dose for dose the mucosal reactions were more intense with barotherapy. The higher doses in oxygen showed mucosal reactions similar to those seen nt the site of a radon implant producing 6000 to 7000-rad tumor doses in 5 to 7 days but of course involved much larger volumes of tissue. The reduced dosage was well tolerated, being no worse than that expected when conventional techniques were used to deliver 6000 to 6500-rad tumor doses in 5 to 6 weeks with 4-Mev x rays. Reduction of the dose to 3 x 1000-rad maximum tumor dose did not significantly alter the sequelae and more recently a maximum tumor dose of 3 x 800 rad was used. Immediate tumor resolution was good but severe radiation reactions required reduction of the dosagn first used. Cases treated during the more » first 10 months are reported in relation to their status from 2 months after treatment. Each patient received general anesthesia, bilateral myringotomy, and pressurization of oxygen to 45 lb/in./sup 2/ gauge pressure in a pressure vessel. Results are reported for 110 cases of locally advanced malignant tumors in various sites that have received treatment combining oxygen barotherapy with 4-Mev x-ray therapy, delivering three large fractions of x-ray dosage in a total time of 21 days. = ,Īttempts were made to develop a radiotherapy technique to increase the sensitivity of various types of tumors by exposing the patient to oxygen at high pressure in a specially constructed chamber while undergoing high-voltage x-ray treatment. ![]() Favorable results are described in patients with urinary bladder tumors administered l50- to 200-rad daily doses, for a total of 6000 to 8000 rads over 6 to 8 weeks. Various technical problems of Co/sup 60/ therapy are discussed, including precise localization of the tumor, calculation of dosage, use of filters to evenly distribute radiation and prevent hot spots, immobilization and positioning of the patient, and direct dosimetry for affirmation of calculated dosage. Some tumors at limited skin depth, such as in the larynx, are not amenable to Co/sup 60/ therapy because of the high exit dose. As a disadvantage, possibility of injury to adjacent organs is greater with Co/ sup 60/ therapy, since skin reactions, indicative of overdosage with x-ray therapy, may be absent. The advantages of Co/sup 60/ therapy over conventional x-ray therapy, stemming from the fact that in the lst instance energy absorption within the tissues is by the Compton effect and in the 2nd case by the photoelectric effect, are: (1) increased skin tolerance, (2) reduced bone absorption, (3) increase in depth dose, (4) diminished radiation sickness, and (5) simplicity of operation. 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